HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 18952118, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Lead diacetate trihydrate | HCID 22456 | — |
| Reactant | HCID 18952303 | HCID 18952303 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18952118 | HCID 18952118 | — |
Reaction Steps
A mixture of 1-(5-fluoro-2-morpholinophenyl)thiourea (5.1 g) suspended in water (36.5 ml), lead acetate trihydrate (7.95 g) in water (36 ml) and potassium hydroxide (11.45 g) in water (32 ml) was heated under reflux for 25 minutes to give N-(5-fluoro-2-morpholinophenyl)cyanamide as a white solid (m.p. 168°-170° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223498 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-28fb1798bade4dcfb074dc2bef24dbe2 |
| Source note | uspto-grants-1993_06 |