HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethoxyphenol → HCID 19754876, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethoxyphenol | HCID 12150 | — |
| Reactant | HCID 19754886 | HCID 19754886 | — |
| Solvent | 2,4,6-Trimethylpyridine | HCID 7953 | — |
| Product | HCID 19754876 | HCID 19754876 | — |
Reaction Steps
The reaction and workup are carried out in the same manner as described for Example 1 using p-bromobenzoic acid N-isopropyl-N-cyclohexyl amide (1.75g, 5.40 mmol), 4-ethoxy phenol (796 mg, 5.76 mmol) and cuprous oxide (390 mg, 2.73 mmol) in collidine (15 ml). The crude product is chromatographed on silica gel using mixtures of ethyl acetate and hexane as eluents to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223539 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-5d09d660ffdc4e2e831eabcf8fc72ec3 |
| Source note | uspto-grants-1993_06 |