HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(3-Aminophenyl)-1-(phenylmethyl)-2-piperazinecarboxamide → 4-(3-Aminophenyl)-2-piperazinecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(3-Aminophenyl)-1-(phenylmethyl)-2-piperazinecarboxamide | HCID 14998814 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(3-Aminophenyl)-2-piperazinecarboxamide | HCID 14998818 | — |
Reaction Steps
To methanol add 4-(3-aminophenyl)-1-(phenylmethyl)-2-piperazinecarboxamide and Pd(OH)2. Place the reaction on a Parr hydrogenator at 50 psi of H2 and shake. Monitor the progress of the reaction by thin-layer chromatography. Upon completion of the reaction, remove the catalyst by suction filtration through celite. Remove solvent in vacuo to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223623 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-21176ba0ae824e138dc70f5be1060c36 |
| Source note | uspto-grants-1993_06 |