HRID1588993
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To methanol add 4-(3-aminophenyl)-1-(phenylmethyl)-2-piperazinecarboxamide and Pd(OH)2. Place the reaction on a Parr hydrogenator at 50 psi of H2 and shake. Monitor the progress of the reaction by thin-layer chromatography. Upon completion of the reaction, remove the catalyst by suction filtration through celite. Remove solvent in vacuo to obtain the title compound.
WORKUP
后处理
- customthe reaction on a Parr hydrogenator at 50 psi of H2 and shake
- customMonitor the progress of the reaction by thin-layer chromatography
- customUpon completion of the reaction
- customremove the catalyst
- filtrationby suction filtration through celite