HRID1588993

反应详情

EQUATION

反应方程式

HRID 1588993 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To methanol add 4-(3-aminophenyl)-1-(phenylmethyl)-2-piperazinecarboxamide and Pd(OH)2. Place the reaction on a Parr hydrogenator at 50 psi of H2 and shake. Monitor the progress of the reaction by thin-layer chromatography. Upon completion of the reaction, remove the catalyst by suction filtration through celite. Remove solvent in vacuo to obtain the title compound.

WORKUP

后处理

  1. customthe reaction on a Parr hydrogenator at 50 psi of H2 and shake
  2. customMonitor the progress of the reaction by thin-layer chromatography
  3. customUpon completion of the reaction
  4. customremove the catalyst
  5. filtrationby suction filtration through celite