HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylonitrile → 1H-1,2,4-Triazole-1-propanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | 1H-1,2,4-Triazole | HCID 9257 | — |
| Product | 1H-1,2,4-Triazole-1-propanamine | HCID 4379682 | — |
Reaction Steps
Acrylonitrile (5) and 1H-1,2,4-triazole (2) are reacted with heat for about 2-4 hours, concentrated to an oil and then hydrogenated with Raney nickel catalyst in methanol and ammonium hydroxide for a period of about 8-10 hours, giving 1H-1,2,4-triazole-1-propanamine (6).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04568685 |
| Source dataset | uspto-grants-1986_02 |
| ORD ID | ord-107dc67aea474d7a9d532df98da20a0b |
| Source note | uspto-grants-1986_02 |