Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Isatoic Anhydride | HCID 8359 | — |
| Reactant | 1H-1,2,4-Triazole-1-propanamine | HCID 4379682 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13588895 | HCID 13588895 | — |
Reaction Steps
A mixture of about 2.5 g of 1H-1,2,4-triazole-1-propanamine, about 3.26 g of isatoic anhydride and about 20 ml of ethanol was heated in an oil bath at about 70° C. for about 30 minutes and then concentrated. The residue was recrystallized from ethyl acetate and the desired product, mp 96°-98° C., was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04568685 |
|---|
| Source dataset | uspto-grants-1986_02 |
|---|
| ORD ID | ord-349cbd8ccec849698bcb934bd5f2207d |
|---|
| Source note | uspto-grants-1986_02 |
|---|
