HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Chloromethyl dodecyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | 1-Dodecanol | HCID 8193 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | Chloromethyl dodecyl ether | HCID 12215332 | — |
Reaction Steps
30 g (1 mole) of paraformaldehyde were stirred in 100 ml 1,2-dichloroethane with 186 g (1 mole) of 1-dodecanol, and HCl gas was passed for 3 hours at 0°-5° C. The product was diluted with more solvent to give a 2M concentration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04568700 |
| Source dataset | uspto-grants-1986_02 |
| ORD ID | ord-51bab49f675c4c66a3ea724ba9a355aa |
| Source note | uspto-grants-1986_02 |