HRID1589236

反应详情

EQUATION

反应方程式

HRID 1589236 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

30 g (1 mole) of paraformaldehyde were stirred in 100 ml 1,2-dichloroethane with 186 g (1 mole) of 1-dodecanol, and HCl gas was passed for 3 hours at 0°-5° C. The product was diluted with more solvent to give a 2M concentration.

WORKUP

后处理

  1. additionThe product was diluted with more solvent
  2. customto give
  3. concentrationa 2M concentration