Formaldehyde → HCID 4547069, compound

HRID 1589237Notes

Reaction equation

HRID 1589237 reaction equation
C=O.[CH3:3][CH:4]1[CH2:9][C@H:8]([OH:10])[C@@H:7]([CH:11]([CH3:13])[CH3:12])[CH2:6][CH2:5]1.[Cl:14][CH:15](Cl)CCl>Cl>[Cl:14][CH2:15][O:10][CH:8]1[CH:7]([CH:11]([CH3:13])[CH3:12])[CH2:6][CH2:5][CH:4]([CH3:3])[CH2:9]1

Participants

5

Reactant 3

HCID 712FormaldehydeHCID 65741,1,2-TrichloroethaneHCID 12285346HCID 12285346, compound

Product 1

HCID 4547069HCID 4547069, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

3.0 g (0.1 mole) of paraformaldehyde were stirred at 0°-5° C. with 15.6 g (0.1 mole) of (+) Menthol in 1,1,2-trichloroethane and HCl gas was passed for 2 hours. The product was further diluted to 1M concentration.

Workup

  1. additionThe product was further diluted to 1M concentration

Sources & evidence

ORD record
ord-474cd678f3d04687a11e172d951be4aa
Source dataset
uspto-grants-1986_02
Patent number
US04568700

Reaction notes

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