HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → Morpholinium, 4-(chloromethylene)-, chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | N-Formylmorpholine | HCID 20417 | — |
| Product | Morpholinium, 4-(chloromethylene)-, chloride | HCID 11355716 | 65.1% |
Reaction Steps
Utilizing a procedure similar that used in Preparation 1, but beginning with N-formylmorpholine (346 gm, 3.01 mol) and phosgene (301 gm, 3.05 mol), a 65% yield (333 gm, 1.96 mol) of N-(chloromethylene)-morpholinium chloride is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04568741 |
| Source dataset | uspto-grants-1986_02 |
| ORD ID | ord-0eae75b19cb7441f88e22943d0a06e5c |
| Source note | uspto-grants-1986_02 |