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Ethanol → H-Leu-Gly-OEt.HCl
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | Leu-Gly | HCID 97364 | — |
| 生成物 | H-Leu-Gly-OEt.HCl | HCID 13334684 | — |
反応手順
To a solution of leucylglycine (5 g, 27 mmol) in 30 ml ethanol cooled to 0° was added SOCl2 (4.1 g, 35 mmol). The reaction solution was stirred overnight at room temperature. The ethanol was removed in vacuo, yielding a glassy product with a consistent mass spectrum, nmr and a single peak in the HPLC.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04569907 |
| 出典データセット | uspto-grants-1986_02 |
| ORD ID | ord-c338b0c6f018486aad287e2750bece4c |
| 出典メモ | uspto-grants-1986_02 |