Hydrochloric Acid → HCID 136387261, compound

HRID 1589496Notes

Reaction equation

HRID 1589496 reaction equation
[C:1]([C:9]1[CH:14]=[C:13]([C:15]#[N:16])[CH:12]=[CH:11][C:10]=1[OH:17])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[ClH:18].[CH2:19]([O:21]CC)C>CO>[ClH:18].[C:1]([C:9]1[CH:14]=[C:13]([CH:15]=[N:16][O:21][CH3:19])[CH:12]=[CH:11][C:10]=1[OH:17])(=[O:8])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 13106793HCID 13106793, compound

Product 1

HCID 136387261HCID 136387261, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

A suspension of 214 g of 2-benzoyl-4-cyanophenol in 1.7 liters of anhydrous methanol was saturated with anhydrous hydrogen chloride, while being cooled in ice and stirred. After having been stirred overnight at room temperature, the mixture was mixed with a large volume of ethyl ether. The precipitated crystals were collected by filtration and dried to yield 156 g of 2-benzoyl-4-methoxyiminomethylphenol hydrochloride.

Workup

  1. temperaturewhile being cooled in ice
  2. stirringAfter having been stirred overnight at room temperature
  3. filtrationThe precipitated crystals were collected by filtration
  4. customdried

Sources & evidence

ORD record
ord-5caa6e42e5fd440e9b51e4104b5bd22c
Source dataset
uspto-grants-1986_02
Patent number
US04570006

Reaction notes

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