Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 20245388 | HCID 20245388 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 14065730 | HCID 14065730 | — |
Reaction Steps
40 Parts by weight of methyl 3-(1',1',2'-trifluoro-2'-chloroethoxy)-benzoate, in a mixture of 8.4 parts by weight of potassium hydroxide, 100 parts by weight of water and 5 parts by weight of tetrahydrofuran, are stirred for 15 minutes at 95° C. The resulting solution is acidified with concentrated hydrochloric acid and the precipitate formed is filtered off and dried; 35 parts of 3-(1',1',2'-trifluoro-2'-chloroethoxy)benzoic acid of melting point 79°-85° C. are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | USRE032087 |
|---|
| Source dataset | uspto-grants-1986_02 |
|---|
| ORD ID | ord-c00542e0e41249ecb8c15ac62ec62155 |
|---|
| Source note | uspto-grants-1986_02 |
|---|
