HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Octene → HCID 620432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Octene | HCID 8125 | — |
| Reactant | Trioctylsilane, 95% | HCID 87780 | — |
| Catalyst | Chlorotris(triphenylphosphine)rhodium(I) | HCID 84599 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 620432 | HCID 620432 | — |
Reaction Steps
A mixture of 2.0 grams trioctylsilane and 10 grams 1-octene in 5 milliliters of toluene was reacted for 2 hours at 75°-80° C. in the presence of 0.009 gram of chlorotris(triphenylphosphine)rhodium(I) to yield 80 weight percent tetraoctylsilane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04572791 |
| Source dataset | uspto-grants-1986_02 |
| ORD ID | ord-05abb628ee924f70bb05e14d3ac0d84c |
| Source note | uspto-grants-1986_02 |