Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 19770953 | HCID 19770953 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19770972 | HCID 19770972 | — |
Reaction Steps
To 0.40 g (1.83 mmol) of ethyl 7-ethylpyrazolo[1,5-a]pyridine-3-carboxylate, 8 ml of 2.5N aq. NaOH solution and 8 ml of ethanol were added, followed by stirring at 100° C. for 8 hours. After the reaction, post treatments were conducted in a similar manner to the syntheses bf the 5-methyl and 2,7-dimethyl derivatives so that crystals were obtained. Yield: 0.34 g (1.79 mmol) (98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05200415 |
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| Source dataset | uspto-grants-1993_04 |
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| ORD ID | ord-411e970b60a749c9aa5326c383e916da |
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| Source note | uspto-grants-1993_04 |
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