HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxide → HCID 22913067, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxide | HCID 961 | — |
| Reactant | Cyanoacetamide | HCID 7898 | — |
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Product | HCID 22913067 | HCID 22913067 | — |
Reaction Steps
reacting ethyl acetoacetate with cyanoacetamide and a hydroxide of an alkali metal, in the presence of an organic solvent, at a temperature of from 60° C. to 80° C., for 1 to 4 hours, to produce 3-cyano-2,6-dihydro-4-methylpyridine;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05200522 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-3192a80db05540f784512e4e32274286 |
| Source note | uspto-grants-1993_04 |