HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19100962, compound → 5-Methyl-octahydropyrrolo(3,4-b)pyrrole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19100962 | HCID 19100962 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-Methyl-octahydropyrrolo(3,4-b)pyrrole | HCID 16228899 | — |
Reaction Steps
10.3 g (47.6 mmol) of 2-benzyl-7-methyl-2,7-diazabicyclo[3.3.0]octane in 200 ml of ethanol are hydrogenated on 2.5 g of palladium/active carbon (10% Pd) at 100° C. and 100 bar. The catalyst is filtered off with suction, the filtrate is concentrated, and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05202337 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-67174bce212c493b97eedae3cd6532e9 |
| Source note | uspto-grants-1993_04 |