HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19100963, compound → HCID 22924370, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19100963 | HCID 19100963 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22924370 | HCID 22924370 | — |
Reaction Steps
4.1 g (19 mmol) of 2-benzyl-4-methyl-2,7-diazabicyclo[3.3.0]octane in 80 ml of methanol are hydrogenated on 1 g of palladium/active carbon (10% Pd) at 100° C. and 100 bar. The catalyst is filtered off, the filtrate is concentrated, and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05202337 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-7cfd6fe38f894d28ae7c202f97feaa49 |
| Source note | uspto-grants-1993_04 |