Ethyl Acrylate → HCID 54414652, compound

HRID 1590550Notes

Reaction equation

HRID 1590550 reaction equation
[C:1]([O:5][CH2:6][CH3:7])(=[O:4])[CH:2]=[CH2:3].[CH3:8][C:9]1[CH:20]=[CH:19][C:12]2[O:13][CH:14]([CH2:17][NH2:18])[CH2:15][O:16][C:11]=2[CH:10]=1>>[CH2:6]([O:5][C:1](=[O:4])[CH2:2][CH2:3][NH:18][CH2:17][CH:14]1[O:13][C:12]2[CH:19]=[CH:20][C:9]([CH3:8])=[CH:10][C:11]=2[O:16][CH2:15]1)[CH3:7]

Participants

3

Reactant 2

HCID 8821Ethyl AcrylateHCID 197675372,3-Dihydro-6-methyl-1,4-benzodioxin-2-methanamine

Product 1

HCID 54414652HCID 54414652, compound

Procedure

4.4 ml (0.04 mol) of ethyl acrylate are added to 7.2 g (0.04 mol) of 6-methylbenzo-1,4-dioxan-2-ylmethylamine and the reaction mixture is left to stand for 60 hours at room temperature, yielding crude 3-[N-(6-methylbenzo-1,4-dioxan-2-ylmethyl)amino]-propionic acid ethyl ester which can be used without further purification.

Workup

  1. waitthe reaction mixture is left

Sources & evidence

ORD record
ord-ddab341ec3e14a0a86e69a70025deaf5
Source dataset
uspto-grants-1993_04
Patent number
US05204334

Reaction notes

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