Ethyl Acrylate → HCID 53654866, compound

HRID 1590551Notes

Reaction equation

HRID 1590551 reaction equation
[C:1]([O:5][CH2:6][CH3:7])(=[O:4])[CH:2]=[CH2:3].[CH3:8][O:9][C:10]1[CH:11]=[CH:12][C:13]2[O:17][CH:16]([CH2:18][NH2:19])[CH2:15][C:14]=2[CH:20]=1>>[CH2:6]([O:5][C:1](=[O:4])[CH2:2][CH2:3][NH:19][CH2:18][CH:16]1[CH2:15][C:14]2[CH:20]=[C:10]([O:9][CH3:8])[CH:11]=[CH:12][C:13]=2[O:17]1)[CH3:7]

Participants

3

Reactant 2

HCID 8821Ethyl AcrylateHCID 34438HCID 34438, compound

Product 1

HCID 53654866HCID 53654866, compound

Procedure

4.4 ml (0.04 mol) of ethyl acrylate are added to 6.5 g (0.04 mol) of 5-methoxy-2,3-dihydrobenzofuran-2-ylmethylamine and the reaction mixture is left to stand for 60 hours at room temperature, yielding 3-[N-(5-methoxy-2,3-dihydrobenzofuran-2-yl)methylamino]-propionic acid ethyl ester in the form of a yellowish oil.

Workup

  1. waitthe reaction mixture is left

Sources & evidence

ORD record
ord-328018fd4be54b75b4ea1efc53200cde
Source dataset
uspto-grants-1993_04
Patent number
US05204334

Reaction notes

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