HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 19767532, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 233963 | HCID 233963 | — |
| Product | HCID 19767532 | HCID 19767532 | — |
Reaction Steps
14.8 g (0.0675 mol) of 6-chloro-2-chloromethylbenzo-1,4-dioxane and 31.0 g of methylamine are heated in a pressure tube for 24 hours at 120°. Evaporating off the excess methylamine and distilling under reduced pressure yield 6-chloro-2-methylaminomethylbenzo-1,4-dioxane having a boiling point of 70°-73° (at 0.001 mbar).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05204334 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-daa819d4eae342d3af1a0312fa989aff |
| Source note | uspto-grants-1993_04 |