HCID 19767732, compound → HCID 14989023, compound

HRID 1590760Notes

Reaction equation

HRID 1590760 reaction equation
[CH2:1]([CH:8]([CH2:14][S:15]([CH:18]1[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1)(=[O:17])=[O:16])[C:9]([O:11]CC)=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>Cl>[CH2:1]([CH:8]([CH2:14][S:15]([CH:18]1[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1)(=[O:16])=[O:17])[C:9]([OH:11])=[O:10])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 19767732HCID 19767732, compound

Product 1

HCID 14989023HCID 14989023, compoundYield 37.5%

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

3.2 g of ethyl 2-(R,S)-benzyl-3-cyclohexylsulfonylpropionate are refluxed in 50 ml of 5 N HCl for 8 hours. The mixture is extracted with dichloromethane, and the extract is dried with Na2SO4. The concentration results in 1.1 g of the title compound as an oil.

Workup

  1. extractionThe mixture is extracted with dichloromethane
  2. dry with materialthe extract is dried with Na2SO4
  3. concentrationThe concentration

Sources & evidence

ORD record
ord-ae6b09f67abb4ae6b380adf46db5684a
Source dataset
uspto-grants-1993_04
Patent number
US05204357

Reaction notes

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