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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1590816Generated: October 30, 2026

Water → HCID 54180567, compound

https://huagongshe.com/reaction/1590816

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantHCID 54068794HCID 54068794—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 54180567HCID 5418056779.7%

Reaction Steps

10% Pd-C (70 mg) was added to a 1% water-containing methanol solution (30 ml) of 2-(N-benzyloxycarbonyl-D-valyl)amino-6-methylbenzoic acid (669 mg), and the mixture was stirred under a hydrogen atmosphere at room temperature for two hours. After the catalyst was filtered off, the filtrate was concentrated to obtain 6-methyl-2-(D-valylamino)benzoic acid (347 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05204462
Source datasetuspto-grants-1993_04
ORD IDord-662fc53128ee4693a9ed7d1c7ff45a94
Source noteuspto-grants-1993_04