HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 54180567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 54068794 | HCID 54068794 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54180567 | HCID 54180567 | 79.7% |
Reaction Steps
10% Pd-C (70 mg) was added to a 1% water-containing methanol solution (30 ml) of 2-(N-benzyloxycarbonyl-D-valyl)amino-6-methylbenzoic acid (669 mg), and the mixture was stirred under a hydrogen atmosphere at room temperature for two hours. After the catalyst was filtered off, the filtrate was concentrated to obtain 6-methyl-2-(D-valylamino)benzoic acid (347 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05204462 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-662fc53128ee4693a9ed7d1c7ff45a94 |
| Source note | uspto-grants-1993_04 |