HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stearoyl chloride → HCID 22463279, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stearoyl chloride | HCID 8212 | — |
| Reactant | 1-Cyclohexyloxy-2,2,6,6-tetramethyl-piperidin-4-ol | HCID 11322811 | — |
| Product | HCID 22463279 | HCID 22463279 | 69% |
Reaction Steps
The title compound is prepared in 69% yield from the reaction of octadecanoyl chloride with 1-cyclohexyloxy-4-hydroxy-2,2,6,6-tetramethylpiperidine following the procedure in Example 17. Purification (Waters Prep. 500A HPLC, 100:1 heptane:ethyl acetate) yields a white solid, m.p. 44°-47° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05204473 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-0692247164564da8baea12e7a7add959 |
| Source note | uspto-grants-1993_04 |