HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Succinate → HCID 19768325, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Succinate | HCID 7820 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 4-Amino-1-cyclohexyloxy-2,2,6,6-tetramethylpiperidine | HCID 22277984 | — |
| Product | HCID 19768325 | HCID 19768325 | 252.3% |
Reaction Steps
A mixture of 1-cyclohexyloxy-4-amino-2,2,6,6-tetramethylpiperidine (2.65 g), dimethyl succinate (1.46 g) and sodium methoxide (50 mg) is heated at 180°-190° C. for 4 hours. The crude product is recrystallized from ethanol/water to afford 1.38 g of the title compound as a white solid, m.p. 230°-34° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05204473 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-53a1246b20654b0a9723fd799fbbb279 |
| Source note | uspto-grants-1993_04 |