HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Cetyl glycidyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1-Chloro-3-(hexadecyloxy)propan-2-ol | HCID 12458859 | — |
| Solvent | Water | HCID 962 | — |
| Product | Cetyl glycidyl ether | HCID 61823 | 60% |
Reaction Steps
To a solution of 3-chloro-2-hydroxypropyl hexadecyl ether (10 g, 0.0311 moles in 20 mls water at 90° C. under argon was added a 50% solution of sodium hydroxide (1.37 g, 0.0343 moles) in 10 mls water over 15 minutes. The reaction was heated under the same conditions for 3 additional hours. Sample was purified by distillation (yield=60%). Upon cooling a white solid formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05206020 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-b74ad81f0a024cbcabd95b46d281b5b4 |
| Source note | uspto-grants-1993_04 |