Hydrochloric Acid → HCID 19766242, compound

HRID 1591171Notes

Reaction equation

HRID 1591171 reaction equation
C([N:9]1[CH2:14][CH2:13][C:12]2([CH2:19][C:18](=[O:20])[C:17]3[CH:21]=[CH:22][CH:23]=[CH:24][C:16]=3[S:15]2)[CH2:11][CH2:10]1)(=O)C1C=CC=CC=1.[ClH:25]>C(O)C>[ClH:25].[NH:9]1[CH2:14][CH2:13][C:12]2([CH2:19][C:18](=[O:20])[C:17]3[CH:21]=[CH:22][CH:23]=[CH:24][C:16]=3[S:15]2)[CH2:11][CH2:10]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19045254HCID 19045254, compound

Product 1

HCID 19766242HCID 19766242, compoundYield 92%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of product from Step C (3.2 g, 0.0095 mol) in ethanol (50 ml) and 6N HCl (50 ml) was heated at reflux. After 18 hours, the reaction was concentrated to dryness and the residue crystallized from ethanol to yield 2.9 g (92%) of product.

Workup

  1. temperatureat reflux
  2. concentrationthe reaction was concentrated to dryness
  3. customthe residue crystallized from ethanol

Sources & evidence

ORD record
ord-8a6552b09a054eb5ab8abae62091b670
Source dataset
uspto-grants-1993_04
Patent number
US05206240

Reaction notes

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