反应详情

500 mgs (3.52 mmol) of 1,2-dimercaptobenzene and 610 mgs (3.00 mmol) of N-benzoyl-4-piperidone were stirred in CH2Cl2 while anhydrous HCl gas was introduced Na2SO4 (2 grams) was added and the mixture stirred 15 hours. The mixture was diluted with CH2Cl2 filtered and washed with H2O, and 10% NaOH. The organics were dried (Na2SO4) and concentrated to a solid (yield 740 mgs).

1. additionwas added
2. filtrationfiltered
3. washwashed with H2O, and 10% NaOH
4. dry with materialThe organics were dried (Na2SO4)
5. concentrationconcentrated to a solid (yield 740 mgs)