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HRID1591430

反应详情

EQUATION

反应方程式

HRID 1591430 的结构方程式

REACTANTS

反应物

2
反应SMILES：CC(C)(C)OC(=O)NCCCC(=O)O
HCID294894

n-boc-gamma-aminobutyric acid

C9H17NO4

反应SMILES：NC1CCc2ccccc2NC1=O
HCID4434433

3-Amino-1,3,4,5-tetrahydro-2H-1-benzazepin-2-one

C10H12N2O

PRODUCTS

产物

1
反应SMILES：CC(C)(C)OC(=O)NCCCC(=O)NC1CCc2ccccc2NC1=O
HCID19025510

未命名化合物

PROCEDURE

实验过程

Prepared from 3-amino-2,3,4,5-tetrahydro-1H-[1]benzazepin-2-one (Example 1, Step A) and 4-(t-butoxycarbonylamino)butyric acid by the procedure described in Example 25, Step A. 1H NMR (200 MHz, CDCl3): 1.42 (s,9H), 1.7-2.1 (m,3H), 2.24 (t,5 Hz,2H), 2.58-3.29 (m,5H), 4.57 (m,1H), 4.86 (br s,1H), 7.0-7.3 (m,4H), 8.32 (s,1H). FAB-MS: calculated for C19H27N3O4 361; found 362 (M+H,60%).