HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethyl bromide → HCID 19766184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethyl bromide | HCID 7666 | — |
| Reactant | 3-Benzyloxycarbonylamino-3-methyl-N-[2,3,4,5-tetrahydro-2-oxo-1H-1-benzazepin-3-yl]-butanamide | HCID 21836609 | — |
| Product | HCID 19766184 | HCID 19766184 | — |
Reaction Steps
Prepared from the intermediate obtained in Step A and 2-phenethyl bromide by the procedure described in Example 3, Step A. 1H NMR (200 MHz, CDCl3): 1.37 (s,6H), 1.68 (m,2H), 2.50 (m,4H), 2.7-3.0 (m,2H), 3.70 (m,1H), 4.48 (m,2H), 5.05 (s,2H), 5.66 (s,1H), 6.99 (m,1H), 7.0-7.4 (m,14H). FAB-MS: calculated for C31H35N3O4 513; found 514 (M+H,100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05206235 |
| Source dataset | uspto-grants-1993_04 |
| ORD ID | ord-917da148e03f4311ae0944ae62cd9204 |
| Source note | uspto-grants-1993_04 |