Hydrochloric Acid → 3,4-Dimethyl-2(3H)-thiazolone hydrazone hydrochloride

HRID 1591509노트

반응식

HRID 1591509 반응식
CC(=[N:4][N:5]=[C:6]1[N:10]([CH3:11])[C:9]([CH3:12])=[CH:8][S:7]1)C.[ClH:13]>>[ClH:13].[CH3:11][N:10]1[C:9]([CH3:12])=[CH:8][S:7][C:6]1=[N:5][NH2:4]

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 734148093,4-Dimethyl-2(3H)thiazolone-(1-methylethylidene)hydrazone

생성물 1

HCID 691153313,4-Dimethyl-2(3H)-thiazolone hydrazone hydrochloride

실험 절차

3.5 g (19 mmol) of 3,4-dimethyl-2(3H)-thiazolone-(1-methylethylidene)hydrazone from step A in 60 mL of 6M hydrochloric acid was heated at 50° C. for 30 minutes. The reaction mixture was then concentrated, and the crude product was recrystallized from ethanol. This gave 2 g (60% of the theoretical) of a pink powder.

후처리

  1. concentrationThe reaction mixture was then concentrated
  2. customthe crude product was recrystallized from ethanol

출처 및 근거

ORD 기록
ord-d56b5d2a15fd4c42b994c3285de05ad0
출처 데이터셋
uspto-grants-2007_11
특허 번호
US07291183B2

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