HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylethylenediamine → HCID 69423830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylethylenediamine | HCID 8014 | — |
| Reactant | Sulfur | HCID 5362487 | — |
| Reactant | HCID 69424047 | HCID 69424047 | — |
| Product | HCID 69423830 | HCID 69423830 | — |
Reaction Steps
Analogously to 13b), 4-[(2,3-dichlorobenzenesulphonyl)methylamino]-N-methyl-N-{2-[4-(1-methyl-4,5-dihydro-1H-imidazol-2-yl)phenyl]ethyl}butyramide was prepared from 0.62 g (1.32 mmol) of N-[2-(4-cyanophenyl)ethyl]-4-[(2,3-dichlorobenzenesulphonyl)methylamino]-N-methylbutyramide, 48 mg (1.49 mmol) of sulphur and 3 ml of N-methylethylenediamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07291642B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-a97933081dc94a6cb31b3b5ceec8bbe3 |
| Source note | uspto-grants-2007_11 |