HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58997692, compound → HCID 58997640, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58997692 | HCID 58997692 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58997640 | HCID 58997640 | 65% |
Reaction Steps
The product from Step h (0.7 g, 1.9 mmol) was dissolved in 100 mL MeOH and added carefully to 0.1 g of 10% Pd/C under N2. The mixture was hydrogenated in a Parr shaker at 50 PSI overnight. Filtration through fiberglass filter paper under N2 and under vacuum yielded 0.45 g of a clear colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07291744B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-380fd544fa844d5eab3d21cc505b0592 |
| Source note | uspto-grants-2007_11 |