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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1592322Generated: October 31, 2026

HCID 58997692, compound → HCID 58997640, compound

https://huagongshe.com/reaction/1592322

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58997692HCID 58997692—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 58997640HCID 5899764065%

Reaction Steps

The product from Step h (0.7 g, 1.9 mmol) was dissolved in 100 mL MeOH and added carefully to 0.1 g of 10% Pd/C under N2. The mixture was hydrogenated in a Parr shaker at 50 PSI overnight. Filtration through fiberglass filter paper under N2 and under vacuum yielded 0.45 g of a clear colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07291744B2
Source datasetuspto-grants-2007_11
ORD IDord-380fd544fa844d5eab3d21cc505b0592
Source noteuspto-grants-2007_11