HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11213457, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 58997671 | HCID 58997671 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 11213457 | HCID 11213457 | 102.6% |
Reaction Steps
The product of Step j (90 mg) and 4N HCl in dioxane (50 mL) were mixed and stirred at room temperature for 3 hours. The reaction was stripped on the rotary evaporator and restripped twice from isopropanol on the rotary evaporator to yield 76 mg of a glass. MS (ESI) detects (M+H)+=466.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07291744B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-95658183d1f34d5a99b188cf2b454c17 |
| Source note | uspto-grants-2007_11 |