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HRID1592442

反应详情

EQUATION

反应方程式

HRID 1592442 的结构方程式

REACTANTS

反应物

3
结构：CN(CCCCN)C(=O)OC(C)(C)C
HCID2756377

tert-Butyl (4-aminobutyl)methylcarbamate

C10H22N2O2

结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

结构：Cc1cnc(C=O)c(C)c1
HCID18731683

3,5-Dimethylpyridine-2-carbaldehyde

C8H9NO

PRODUCTS

生成物

1
结构：Cc1cnc(CNCCCCN(C)C(=O)OC(C)(C)C)c(C)c1
HCID58997083

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Using General Procedure B: Reaction of (4-Amino-butyl)-methyl-carbamic acid tert-butyl ester and 3,5-dimethyl-pyridine-2-carbaldehyde with NaBH(OAc)3 in CH2Cl2 gave {4-[(3,5-Dimethyl-pyridin-2-ylmethyl)-amino]-butyl}-methyl-carbamic acid tert-butyl ester as a colorless oil.