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HRID1592470

反应详情

EQUATION

反应方程式

HRID 1592470 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

结构：Cc1cnc(C=O)c(C)c1
HCID18731683

3,5-Dimethylpyridine-2-carbaldehyde

C8H9NO

结构：CC(C)(N)c1ccccn1
HCID22736922

2-(Pyridin-2-yl)propan-2-amine

C8H12N2

PRODUCTS

生成物

1
结构：Cc1cnc(CNC(C)(C)c2ccccn2)c(C)c1
HCID67272239

未命名化合物

收率 36%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Using General Procedure B: Reaction of 1-methyl-1-pyridin-2-yl-ethylamine, 3,5-dimethylpyridine-2-carbaldehyde and NaBH(OAc)3 in CH2Cl2 gave (3,5-dimethyl-pyridin-2-ylmethyl)-(1-methyl-1-pyridin-2-yl-ethyl)-amine as a light brown oil (94 mg, 36%).