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HRID1592512

反应详情

EQUATION

反应方程式

HRID 1592512 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)NCCCCN
HCID4351

未命名化合物

结构：Cn1ccnc1C=O
HCID139575

1H-Imidazole-2-carboxaldehyde, 1-methyl-

C5H6N2O

PRODUCTS

生成物

1
结构：Cn1ccnc1CNCCCCNC(=O)OC(C)(C)C
HCID67272418

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
溶剂HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

PROCEDURE

实验过程

Using General Procedure B, reaction of 1-methyl-1H-imidazole-2-carbaldehyde and (4-amino-butyl)-carbamic acid tert-butyl ester in CH2Cl2 and NaBH(OAc)3 gave {4-[(1-methyl-1H-imidazol-2-ylmethyl)-amino]-butyl}-carbamic acid tert-butyl ester as a sticky white foam.