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HRID1592537

反应详情

EQUATION

反应方程式

HRID 1592537 的结构方程式

REACTANTS

反应物

3
结构：Cc1cccnc1CN
HCID1514370

(3-Methylpyridin-2-yl)methanamine

C7H10N2

结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

结构：CC(C)(C)OC(=O)N=C(NC(=O)OC(C)(C)C)N1CCC(=O)CC1
HCID67272519

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cccnc1CNC1CCN(C(=NC(=O)OC(C)(C)C)NC(=O)OC(C)(C)C)CC1
HCID67272689

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Using General Procedure B, reaction of [tert-butoxycarbonylimino-(4-oxo-piperidin-1-yl)-methyl]-carbamic acid tert-butyl ester, C-(3-methylpyridin-2-yl)-methylamine and NaBH(OAc)3 in CH2Cl2 gave (tert-butoxycarbonylimino-{4-[(3-methyl-pyridin-2-ylmethyl)-amino]-piperidin-1-yl}-methyl)-carbamic acid tert-butyl ester as a white solid.