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HRID1592644

反应详情

EQUATION

反应方程式

HRID 1592644 的结构方程式

REACTANTS

反应物

3
结构：Cc1cccnc1CN
HCID1514370

(3-Methylpyridin-2-yl)methanamine

C7H10N2

结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

结构：CC(C)(C)OC(=O)Nc1cccnc1C=O
HCID10911130

tert-Butyl (2-formylpyridin-3-yl)carbamate

C11H14N2O3

PRODUCTS

生成物

1
结构：Cc1cccnc1CNCc1ncccc1NC(=O)OC(C)(C)C
HCID67271562

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Using General Procedure B: Reaction of C-(3-methyl-pyridin-2-yl)-methylamine and (2-formyl-pyridin-3-yl)-carbamic acid tert-butyl ester with NaBH(OAc)3 in CH2Cl2 gave (2-{[(3-Methyl-pyridin-2-ylmethyl)-amino]-methyl}-pyridin-3-yl)-carbamic acid tert-butyl ester as a yellow oil.