HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiazole → HCID 69411283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiazole | HCID 9256 | — |
| Reactant | 1-Boc-4-(2-formylphenyl)piperazine | HCID 6490990 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 69411283 | HCID 69411283 | — |
Reaction Steps
Thiazole was lithiated with n-butyllithium and reacted with N-Boc-4-(2-formylphenyl)-piperazine in a manner similar to preparation 113A. The resulting alcohol was deoxygenated in a manner similar to preparation 115A to afford the final compound. LRMS (ESI+): 360.1 (M+1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07291619B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-0e86953e25c04b138611cfa183107bce |
| Source note | uspto-grants-2007_11 |