HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Tetrazole, 1-methyl- → HCID 69409082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Tetrazole, 1-methyl- | HCID 140123 | — |
| Reactant | 1-Boc-4-(2-formylphenyl)piperazine | HCID 6490990 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 69409082 | HCID 69409082 | — |
Reaction Steps
1-methyltetrazole was lithiated with n-butyllithium and reacted with N-Boc-4-(2-formylphenyl)-piperazine in a manner similar to preparation 113A. The resulting alcohol was deoxygenated in a manner similar to preparation 115A to afford the final compound. LRMS (ESI+): 358.3 (M+1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07291619B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-6e26a5557556495a91f087605939faac |
| Source note | uspto-grants-2007_11 |