HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69410555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 69410556 | HCID 69410556 | — |
| Product | HCID 69410555 | HCID 69410555 | — |
Reaction Steps
Into a flask containing (R)-N-{1-(4-chlorobenzyl)-2-oxo-2-[4-(2-([1,2,4]triazol-1-yl)methylphenyl)-piperazin-1-yl]-ethyl}-2-(2-isopropyl-2,3-dihydro-1H-isoindol-1-yl)-acetamide (Example 162) was added 1.0 N HCl (5 mL). After about an hour, the solution was solidified at −78° C., and the solid lyophilized to give about 0.06 g of the final compound as tan solids. ES MS 626.3 (M+H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07291619B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-1b762a1707264d7faa457683e697c4fc |
| Source note | uspto-grants-2007_11 |