HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 25248372, compound → HCID 19627217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 25248372 | HCID 25248372 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19627217 | HCID 19627217 | — |
Reaction Steps
2-Fluoro-4-nitro-1-phenoxybenzene and 7.2 g of 10% Pd/C were dissolved in 200 mL EtOH and stirred under 1 atmosphere of H2 overnight. The reaction mixture was filtered through Celite with the aid of 50 mL EtOH and concentrated to provide 3-fluoro-4-phenoxybenzenamine as an oil which was used in Step C without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07294616B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-59ba03bb420749c99fbb16526e42678d |
| Source note | uspto-grants-2007_11 |