HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69414044, compound → HCID 9978315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69414044 | HCID 69414044 | — |
| Reactant | HCID 69415264 | HCID 69415264 | — |
| Product | HCID 9978315 | HCID 9978315 | 78.1% |
Reaction Steps
The reaction was carried out in the same manner as in Example 8-2) except for using 659 mg (1.32 mmol) of 4-{2-[(t-butoxycarbonyl)ethylamino]pyridin-4-yl}-3-(4-fluorophenyl)-1-([1,2,4]triazolo[4,3-b]pyridazin-6-yl)-1H-pyrazole obtained in Example 14-1) in place of 4-(2-t-butoxycarbonylaminopyridin-4-yl)-3-(4-fluorophenyl)-1-([1,2,4]triazolo[4,3-b]pyridazin-6-yl)-1H-pyrazole to obtain 413 mg of the title compound as a beige powder. (Yield: 78%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07294625B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-76113f0bda794956a3dff681ecd03332 |
| Source note | uspto-grants-2007_11 |