HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-t-Butoxycarbonylaminopyridin-4-yl)-3-dimethylamino-1-phenyl-2-propen-1-one → HCID 178452638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-t-Butoxycarbonylaminopyridin-4-yl)-3-dimethylamino-1-phenyl-2-propen-1-one | HCID 69414152 | — |
| Reactant | 2-(2-t-Butoxycarbonylaminopyridin-4-yl)-3-dimethylamino-1-(4-fluorophenyl)-2-propen-1-one | HCID 69415993 | — |
| Product | HCID 178452638 | HCID 178452638 | 86% |
Reaction Steps
The reaction was carried out in the same manner as in Example 2-2) except for using 18.4 g (50.0 mmol) of 2-(2-t-butoxycarbonylaminopyridin-4-yl)-3-dimethylamino-1-phenyl-2-propen-1-one obtained in Example 20-1) in place of 2-(2-t-butoxycarbonylaminopyridin-4-yl)-3-dimethylamino-1-(4-fluorophenyl)-2-propen-1-one to obtain 14.5 g of the title compound as a white powder. (Yield: 86%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07294625B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-5e48ee8918f544b2b3a5ccecf7cc0d24 |
| Source note | uspto-grants-2007_11 |