HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-t-Butoxycarbonylaminopyridin-4-yl)-1-(4-chlorophenyl)-3-dimethylamino-2-propen-1-one → HCID 178452641, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-t-Butoxycarbonylaminopyridin-4-yl)-1-(4-chlorophenyl)-3-dimethylamino-2-propen-1-one | HCID 69413431 | — |
| Reactant | 2-(2-t-Butoxycarbonylaminopyridin-4-yl)-3-dimethylamino-1-(4-fluorophenyl)-2-propen-1-one | HCID 69415993 | — |
| Product | HCID 178452641 | HCID 178452641 | 97% |
Reaction Steps
The reaction was carried out in the same manner as in Example 2-2) except for using 10.1 g (25.0 mmol) of 2-(2-t-butoxycarbonylaminopyridin-4-yl)-1-(4-chlorophenyl)-3-dimethylamino-2-propen-1-one obtained in Example 23-1) in place of 2-(2-t-butoxycarbonylaminopyridin-4-yl)-3-dimethylamino-1-(4-fluorophenyl)-2-propen-1-one to obtain 9.01 g of the title compound as a pale yellowish white powder. (Yield: 97%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07294625B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-49bd705f3e644a0b9df1294f129a03b6 |
| Source note | uspto-grants-2007_11 |