HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl acetoacetate → HCID 58999174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl acetoacetate | HCID 7757 | — |
| Reactant | 1-(Aminomethyl)cyclohexan-1-ol | HCID 77614 | — |
| Reactant | HCID 11150335 | HCID 11150335 | — |
| Product | HCID 58999174 | HCID 58999174 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 68, using 3-oxo-butyric acid methyl ester as compound of formula R, 2-bromo-1-(2,4-dichloro-5-fluorophenyl)-ethanone as compound of formula S, c-cyclohexyl-methylamine as R3—(CH2)m—NH2 and 1-aminomethyl-1-cyclohexanol as R1R2NH, MS (ISP) 495.5 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07294644B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-18e0970acae04505a74522daa99e030c |
| Source note | uspto-grants-2007_11 |