N,N-Dimethylethylenediamine → HCID 69433451, compound

Participants

Reaction Steps

The title compound (0.03 g, 20%) was prepared from the product of Example 7 Step 6 and N,N-dimethylethylenediamine using the method of Example 7 Step 7; 1H NMR (CDCl3) 8.68 (2H, s), 8.52 (2H, d, J 8 Hz), 7.82 (1H, d, J 10 Hz), 7.57 (H, s), 7.46 (1H, d, J 10 Hz), 7.39 (2H, J 8 Hz), 6.67 (1H, s), 5.90 (1H, m), 3.53 (2H, m), 3.18 (2H, t, J 5 Hz), 2.77 (2H, t, J 8 Hz,), 2.56 (2H, t, J 5 Hz) 2.29 (6H, s).

Provenance & Evidence