4-Pyridinecarboxaldehyde → HCID 86595417, compound

HRID 1593434Notes

Reaction equation

HRID 1593434 reaction equation
[CH3:1][O:2][N:3]=[C:4]1[C:12]2[C:7](=[CH:8][C:9](/[CH:13]=[CH:14]/[C:15]([C:17]3[CH:22]=[CH:21][C:20]([O:23][CH3:24])=[CH:19][CH:18]=3)=[O:16])=[CH:10][CH:11]=2)[CH2:6][CH2:5]1.[N:25]1[CH:30]=[CH:29][C:28]([CH:31]=[O:32])=[CH:27][CH:26]=1>>[CH3:1][O:2][N:3]=[C:4]1[C:12]2[C:7](=[CH:8][C:9]([CH:13]([CH2:14][C:15]([C:17]3[CH:18]=[CH:19][C:20]([O:23][CH3:24])=[CH:21][CH:22]=3)=[O:16])[C:31]([C:28]3[CH:29]=[CH:30][N:25]=[CH:26][CH:27]=3)=[O:32])=[CH:10][CH:11]=2)[CH2:6][CH2:5]1

Participants

3

Reactant 2

HCID 133894-PyridinecarboxaldehydeHCID 86595416HCID 86595416, compound

Product 1

HCID 86595417HCID 86595417, compoundYield 86%

Procedure

The title compound (8.82 g, 86%) was prepared from the product of Step 1 and pyridine-4-carboxaldehyde fusing the method of Example 1 Step 4; MS(ES+) m/e 429 [M+H]+.

Sources & evidence

ORD record
ord-1cc337c6d2dc4a5c914a65544094c894
Source dataset
uspto-grants-2007_11
Patent number
US07297694B2

Reaction notes

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