HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridinecarboxaldehyde → 4-{4-[3-(1-Methoxyiminoindan-5-yl)4-oxo-4-pyridin-4-ylbutanoyl]phenoxy}piperidine-1-carboxylic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | 4-{4-[(E)-3-(1-Methoxyimino-indan-5-yl)allanoyl]phenoxy}piperidine-1-carboxylic acid tert-butyl ester | HCID 86595418 | — |
| Product | 4-{4-[3-(1-Methoxyiminoindan-5-yl)4-oxo-4-pyridin-4-ylbutanoyl]phenoxy}piperidine-1-carboxylic acid tert-butyl ester | HCID 86595419 | 88% |
Reaction Steps
The title compound (0.9 g, 88%) was prepared from the product of Step 2 and pyridine-4-carboxaldehyde using the method of Example 1 Step 4; MS(ES+) m/e 597 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07297694B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-b3c2850a2cef4b099efa1e0e0a8b550e |
| Source note | uspto-grants-2007_11 |